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Yuxiang Wen, Wei Ji, Jiang Yu, Qichang An, Tianfen Qin, Zhiya Zhang, Jiachi Zhang, Shanglong Peng
Charact. Appl. Nanomater.
2020
,
3(1);
840 Views
Abstract
BiVO 4 was hydrothermally synthesized under different preparing conditions and characterized by XRD, SEM, Raman spectrum and BET specific surface area. The influence of different pH value and annealing temperature and hydrothermal time on the morphologies and structures of the BiVO 4 samples was investigated systematically. It can be found that annealing would eliminate the effects caused by the pH of precursor, heating temperature and heating time, but preparing conditions still influenced the size and specific surface area of samples. Furthermore, the photocatalytic activities of the fabricated BiVO 4 were also evaluated by the degradation of methyl blue in aqueous solution under UV and visible light irradiation.
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Simge Gencalp Irizalp, Nursen Saklakoglu
Charact. Appl. Nanomater.
2020
,
3(1);
802 Views
Abstract
In this study, nano-scale microstructural evolution in 6061-T6 alloy after laser shock processing (LSP) was studied. 6061-T6 alloy plate was subjected to multiple LSP. The LSP treated area was characterized by X-ray diffraction and the microstructure of the samples was analyzed by transmission electron microscopy. Focused Ion Beam (FIB) tools were used to prepare TEM samples in precise areas. It was found that even though aluminum had high stacking fault energy, LSP yielded to formation of ultrafine grains and deformation faults such as dislocation cells, stacking faults. The stacking fault probability (PSF) was obtained in LSP-treated alloy using X-Ray diffraction. Deformation induced stacking faults lead to the peak position shifts, broadening and asymmetry of diffraction. XRD analysis and TEM observations revealed significant densities of stacking faults in LSP-treated 6061-T6 alloy. And mechanical properties of LSP-treated alloy were also determined to understand the hardening behavior with high concentration of structural defects.
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Alexander Yu. Vasil’kov, Alexander V. Budnikov, Alexander V. Naumkin
Charact. Appl. Nanomater.
2020
,
3(1);
670 Views
Abstract
New hybrid magnetic materials based on HDPE filled with Со and Ni nanoparticles have been prepared via the metal vapor synthesis. Properties of the metal-polymer composites have been elucidated as a function of MVS parameters and metal nature. The Faraday method has been applied to characterize the magnetic properties of the systems. The microstructure of the samples has been studied with a number of X-ray and synchrotron techniques, including XRD, EXAFS and SAXS. Core-level and valence band spectra were measured by XPS. The peak at binding energy of 282.8 eV characteristic of C-Ni bond was recorded in the C 1s spectrum. It was shown that properties of nanocomposite materials with similar compositions are determined both by the synthesis conditions and post-synthesis factors.
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Kalyan Adhikary, Sayan Das, Debasish De, Anup Mondal, Utpal Gangopadhyay, Sukhendu Jana
Charact. Appl. Nanomater.
2020
,
3(1);
1356 Views
Abstract
Diamond-like Nanocomposites (DLN) is a newly member in amorphous carbon (a:C) family. It consists of two or more interpenetrated atomic scale network structure s . The amorphous silicon oxide (a:SiO) is incorporated within diamond-like carbon (DLC) matrix i.e. a:CH and both the network is interpenetrated by Si-C bond. Hence, the internal stress of deposited DLN film decreases remarkably compare to DLC. The diamond - like properties ha ve come due to deform tetrahedral carbon with sp 3 configuration and high ratio of sp 3 to sp 2 bond. The DLN has excellent mechanical, electrical, optical and tribological properties. Those properties of DLN could be varied over a wide range by changing deposition parameters, precursor and even post deposition treatment also. The range of properties are: Resistivity 10 -4 to 10 14 Ωcm, hardness 10–22 GPa, coefficient of friction 0.03-0.2, wear factor 0.2-0.4 10 -7 mm 3 /Nm, transmission Vis - far IR, modulus of elasticity 150-200 GPa, residual stress 200-300 Mpa, d ielectric constant 3-9 and maximum operating temperature 600 ° C in oxygen environment and 1200 ° C in O 2 free air. Generally, the PECVD method is used to synthesi ze the DLN film. The most common procedures used for investigation of structure and composition of DLN films are Raman spectroscopy, Fourier transformed infrared spectroscopy (FTIR), HRTEM, FESEM and X-ray photo electron spectroscopy (XPS). Interest in the coating technology has been expressed by nearly every industrial segment including automotive, aerospace, chemical processing, marine, energy, personal care, office equipment, electronics, biomedical and tool and die or in a single line from data to beer in all segment of life. In this review paper, characterization of d iamond-like n anocomposites is discussed and subsequently different application areas are also elaborated.
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Sajad Hussain Din, M. A. Shah, N. A. Sheikh, M. Mursaleen Butt
Charact. Appl. Nanomater.
2020
,
3(1);
2982 Views
Abstract
Nanocomposites are high performance materials which reveal rare properties. Nanocomposites have an estimated annual growth rate of 25% and fastest demand to be in engineering plastics and elastomers. Their prospective is so prominent that they are valuable in numerous areas ranging from packaging to biomedical applications. In this review , the various types of matrix nanocomposites are discussed highlighting the need for these materials, their processing approaches and some recent results on structure, properties and potential applications. Perspectives includ e need for such future materials and other interesting applications. Being environmentally friendly, applications of nanocomposites propose new technology and business opportunities for several sectors of the aerospace, automotive, electronics and biotechnology industries.
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